Routine Maintenance
As with any piece of instrumentation or equipment, there are many aspects of maintenance that need to be encompassed by daily, weekly and annual procedures. The frequency of maintenance is typically determined by the sample volume and cumulative run time that the instrument is subjected to.
One of the first things that should be carried out before the calibration of the ICP-MS is a sensitivity check and optimization. This ensures that the operator is aware of any possible issues with the instrument and if so, may address them before beginning a calibration. Typical indicators of sensitivity are Rhodium levels, Cerium/Oxide ratios and DI water blanks.
One of the most frequent forms of routine maintenance is replacing sample and waste tubing on the peristaltic pump, as these tubes can get worn fairly quickly resulting in holes and clogs in the sample line, resulting in skewed results. Other parts that will need regular cleaning and/or replacing are sample tips, nebulizer tips, sample cones, skimmer cones, injector tubes, torches and lenses. It may also be necessary to change the oil in the interface roughing pump as well as the vacuum backing pump, depending on the workload put on the instrument.
Read more about this topic: Inductively Coupled Plasma Mass Spectrometry
Famous quotes containing the words routine and/or maintenance:
“An entertainment is something which distracts us or diverts us from the routine of daily life. It makes us for the time being forget our cares and worries; it interrupts our conscious thoughts and habits, rests our nerves and minds, though it may incidentally exhaust our bodies. Art, on the other hand, though it may divert us from the normal routine of our existence, causes us in some way or other to become conscious of that existence.”
—Sir Herbert Read (1893–1968)
“However patriarchal the world, at home the child knows that his mother is the source of all power. The hand that rocks the cradle rules his world. . . . The son never forgets that he owes his life to his mother, not just the creation of it but the maintenance of it, and that he owes her a debt he cannot conceivably repay, but which she may call in at any time.”
—Frank Pittman (20th century)